Paper Title
Environmentally Microwave Assisted Synthesis and Characterization of Bio-inorganic Material with Co(II)
Article Identifiers
: Authors
Keywords
bio-inorganic material, P-Iodo Isonitroso Acetophenone (P-IINAP), Elemental analysis, Magnetic measurements, Octahedral Geometry, 1H-NMR, Infrared.
Abstract
In the present investigation we synthesized and characterized the bio-inorganic material complex Co(II) of P- Iodo Isonitroso Acetophenone (P-IINAP) were synthesized from p-Iodo Acetophenone and characterized by on the basis of elemental analysis, molecular weight determination and molar conductance data. The bio-inorganic material of Schiff bases are widely studied because of the increasing recognition of their role in biological systems. Schiff bases and their complexes were recently found to have significant antitumor and biological activity. The isolated bio-inorganic materials of Schiff base behave as non-electrolyte in DMF solution. The electronic spectral data for ligand p-IINAP and complexes of Schiff base shows a group of three or more bands in the range 220 - 320 nm, which can be attributed to π-π* transition and charge transfer transition. Infrared spectra (4000-400cm-1) of the bio-inorganic materials are practically identical. The frequencies of some significant bands of the free ligand around 3320-3340cm-1 due to hydrogen bonded –OH of =N-OH stretching. The absence of –OH stretching frequencies in the Co(II) complex indicates that the hydrogen of oxime group is replaced by transition metal ions on complex formation. The 1H- NMR spectrum of bio-inorganic material in DMSO solution observed a peak due to different types of protons. The Magnetic measurements indicate that the complexes are Paramagnetic. The results indicate that the transition metal complex of Co(II) is hexa- coordinated and Octahedral Geometry.
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How To Cite (APA)
R. G. Mahakale, R. G. Gajbhiye, & T. D. Kose (September-2023). Environmentally Microwave Assisted Synthesis and Characterization of Bio-inorganic Material with Co(II). INTERNATIONAL JOURNAL OF NOVEL RESEARCH AND DEVELOPMENT, 8(9), a509-a514. https://ijnrd.org/papers/IJNRD2309062.pdf
Issue
Volume 8 Issue 9, September-2023
Pages : a509-a514
Other Publication Details
Paper Reg. ID: IJNRD_204926
Published Paper Id: IJNRD2309062
Downloads: 000122255
Research Area: Chemistry
Author Type: Indian Author
Country: Wardha, Maharashtra, India
Published Paper PDF: https://ijnrd.org/papers/IJNRD2309062.pdf
Published Paper URL: https://ijnrd.org/viewpaperforall?paper=IJNRD2309062
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