Environmentally Microwave Assisted Synthesis and Characterization of Bio-inorganic Material with Co(II)

Environmentally Microwave Assisted Synthesis and Characterization of Bio-inorganic Material with Co(II)

Registration ID: IJNRD_204926

Published ID: IJNRD2309062

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R. G. Mahakale , R. G. Gajbhiye , T. D. Kose

bio-inorganic material, P-Iodo Isonitroso Acetophenone (P-IINAP), Elemental analysis, Magnetic measurements, Octahedral Geometry, 1H-NMR, Infrared.

In the present investigation we synthesized and characterized the bio-inorganic material complex Co(II) of P- Iodo Isonitroso Acetophenone (P-IINAP) were synthesized from p-Iodo Acetophenone and characterized by on the basis of elemental analysis, molecular weight determination and molar conductance data. The bio-inorganic material of Schiff bases are widely studied because of the increasing recognition of their role in biological systems. Schiff bases and their complexes were recently found to have significant antitumor and biological activity. The isolated bio-inorganic materials of Schiff base behave as non-electrolyte in DMF solution. The electronic spectral data for ligand p-IINAP and complexes of Schiff base shows a group of three or more bands in the range 220 - 320 nm, which can be attributed to π-π* transition and charge transfer transition. Infrared spectra (4000-400cm-1) of the bio-inorganic materials are practically identical. The frequencies of some significant bands of the free ligand around 3320-3340cm-1 due to hydrogen bonded –OH of =N-OH stretching. The absence of –OH stretching frequencies in the Co(II) complex indicates that the hydrogen of oxime group is replaced by transition metal ions on complex formation. The 1H- NMR spectrum of bio-inorganic material in DMSO solution observed a peak due to different types of protons. The Magnetic measurements indicate that the complexes are Paramagnetic. The results indicate that the transition metal complex of Co(II) is hexa- coordinated and Octahedral Geometry.

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"Environmentally Microwave Assisted Synthesis and Characterization of Bio-inorganic Material with Co(II)", IJNRD - INTERNATIONAL JOURNAL OF NOVEL RESEARCH AND DEVELOPMENT (www.IJNRD.org), ISSN:2456-4184, Vol.8, Issue 9, page no.a509-a514, September-2023, Available :https://ijnrd.org/papers/IJNRD2309062.pdf

Volume 8 Issue 9, September-2023

Pages : a509-a514

Paper Reg. ID: IJNRD_204926

Published Paper Id: IJNRD2309062

Downloads: 000121144

Research Area: Chemistry

Country: Wardha, Maharashtra, India

Published Paper PDF: https://ijnrd.org/papers/IJNRD2309062.pdf

Published Paper URL: https://ijnrd.org/viewpaperforall?paper=IJNRD2309062

Journal Name: INTERNATIONAL JOURNAL OF NOVEL RESEARCH AND DEVELOPMENT(IJNRD)

ISSN: 2456-4184 | IMPACT FACTOR: 8.76 Calculated By Google Scholar | ESTD YEAR: 2016

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