Paper Title
Microwave-assisted synthesis of lead sulfide (PbS) nanostructures from a newly single molecular precursor
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Microwave-assisted synthesis of lead sulfide (PbS) nanostructures from a newly single molecular precursor
Abstract
Lead sulfide nanostructures were synthesized by microwave irradiation of S-methyl dithiocarbazate lead (II) complex precursor in DMSO. Lead sulfide nanostructures were characterized using X-ray diffraction (XRD), Fourier transform infrared spectra (FTIR),transmission electron microscopy (TEM),scanning electron microscopy(SEM) .The optical properties of these samples were examine by UV-visible and photoluminescence spectroscopy. The band gap energy were obtained as 1.12 and 1.15 eV for the nano-rods and nano-cubes respectively, a blue shift from the bulk value (0.4 eV) which could be ascribed to quantum confinement effect. The result established the significant effect of the precursor type on the morphologies of the PbS.
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How To Cite (APA)
Arvind Kumar, D. Kumar, Upendra K.Ttipathi, & Rayees A. Bhat (January-2023). Microwave-assisted synthesis of lead sulfide (PbS) nanostructures from a newly single molecular precursor. INTERNATIONAL JOURNAL OF NOVEL RESEARCH AND DEVELOPMENT, 8(1), a314-a322. https://ijnrd.org/papers/IJNRD2301037.pdf
Issue
Volume 8 Issue 1, January-2023
Pages : a314-a322
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Paper Reg. ID: IJNRD_185528
Published Paper Id: IJNRD2301037
Downloads: 000121993
Research Area: Engineering
Author Type: Foreign Author
Country: -, -, -
Published Paper PDF: https://ijnrd.org/papers/IJNRD2301037.pdf
Published Paper URL: https://ijnrd.org/viewpaperforall?paper=IJNRD2301037
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